1,3,5-三异丙基苯合成路线 （共 123 条）
反应条件
T=0°C; Lichtausschluss;
参考文献
Fuson; Horning
Journal of the American Chemical Society, 1940 , vol. 62, p. 2962
Full Text View citing articles Show Details
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: 99.6 g / AlCl3 / CS2 / 1 h / Heating 2: LiAlH4 / diethyl ether / 2 h / Heating 3: 165.0 g / N,N-dimethylaminopyridine / pyridine / 2 h / 100 - 110 °C 5: aq. KOH / methanol / 2.5 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 7, # 9 p. 2707 - 2710
反应条件
1: aqueous NaOH; oxygen
2: aqueous Na2SO3
View Scheme
参考文献
Seidel et al.
Journal fuer Praktische Chemie (Leipzig), 1956 , vol. <4> 3, p. 278,297
Full Text Show Details
Wolkow; Sawgorodnii
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3672,3676; engl. Ausg. S. 3630, 3633
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile
T=75°C; P=760 Torr; 2 h;
2: With sulfuric acid in acetonitrile
T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Aoki, Yasuhiro; Hirai, Naruhisa; Sakaguchi, Satoshi; Ishii, Yasutaka
Tetrahedron, 2005 , vol. 61, # 46 p. 10995 - 10999
反应条件
1: air; aqueous Na2CO3
2: HClO4; acetic acid
View Scheme
参考文献
Hooker Electrochem. Co.
Patent: US2790010 , 1952 ;
参考文献
Hooker Electrochem. Co.
Patent: US2790010 , 1952 ;
反应条件
titanium tetrachloride in dichloromethane
12 h;
参考文献
Anderson, Sven; Carter, Robert E.; Drakenberg, Torbjoern
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 7 p. 579 - 596
反应条件
hydrogenchloride; tetrachloroethane, 1,1,2,2-
Versetzen mit AlCl3 bei 0grad, mehrstuendiges Einleiten von HCl bei 70grad und Behandeln mit wss. HCl, zuletzt bei Siedetemperatur;
参考文献
Fuson et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 30,31
Org. Synth. Coll., 1955 , vol. Vol. III, p. 549,551
参考文献
Fuson et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 30,31
Org. Synth. Coll., 1955 , vol. Vol. III, p. 549,551
反应条件
disulfur dichloride; acetic acid; zinc(II) chloride
T=20 - 60°C; 25 h; Inert atmosphere;
参考文献
UBE INDUSTRIES, LTD.
Patent: US2012/157716 A1, 2012 ;
Location in patent: Page/Page column 4-5 ;
