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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
717101-32-1
合成路线
（共 10 条）
696-62-8
4-碘苯甲醚
+
1206164-21-7
→
反应条件
717101-32-1
反应条件
copper(l) iodide; 1,10-phenanthroline in N,N-dimethyl acetamide T=160°C; 24 h; Inert atmosphere;
参考文献
Shang, Rui; Fu, Yao; Wang, Yan; Xu, Qing; Yu, Hai-Zhu; Liu, Lei
Angewandte Chemie - International Edition, 2009 , vol. 48, # 49 p. 9350 - 9354
623-12-1
4-氯苯甲醚
+
1206164-21-7
→
反应条件
717101-32-1
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in diethylene glycol dimethyl ether T=160°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
104-92-7
4-溴苯甲醚
+
1206164-21-7
→
反应条件
717101-32-1
反应条件
palladium diacetate; tris-(o-tolyl)phosphine in diethylene glycol dimethyl ether T=160°C; 24 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
213596-33-9
+
385-00-2
2,6-二氟苯甲酸
→
反应条件
717101-32-1
反应条件
palladium (II) trifluoroacetate; silver carbonate in dimethyl sulfoxide T=120°C; Suzuki coupling; 2 h;
参考文献
Dai, Jian-Jun; Liu, Jing-Hui; Luo, Dong-Fen; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 2 p. 677 - 679
104-92-7
4-溴苯甲醚
+
1206164-21-7
→
反应条件
717101-32-1
+
2132-80-1
4,4-二甲氧基联苯
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in diethylene glycol dimethyl ether T=160°C; 24 h; Inert atmosphere;
参考文献
Shang, Rui; Xu, Qing; Jiang, Yuan-Ye; Wang, Yan; Liu, Lei
Organic Letters, 2010 , vol. 12, # 5 p. 1000 - 1003
104-92-7
4-溴苯甲醚
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
623-12-1
4-氯苯甲醚
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
66107-29-7
4-甲氧基三氟甲烷磺酸苯酯
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
372-18-9
1,3-二氟苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
717101-32-1
+
90101-30-7
2,4-二氟-4'-甲氧基-1,1'-联苯
反应条件
potassium phosphate; palladium diacetate; silver carbonate; 2,2,2-trimethylacetic acid in dimethylammonium 2,4-dichlorophenoxyacetate T=120°C; 10 h;
参考文献
Wei, Ye; Kan, Jian; Wang, Min; Su, Weiping; Hong, Maochun
Organic Letters, 2009 , vol. 11, # 15 p. 3346 - 3349
623-12-1
4-氯苯甲醚
+
5720-06-9
2-甲氧基苯基硼酸
+
162101-25-9
2,6-二氟苯硼酸
→
反应条件
717101-32-1
+
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; 2nd generation X-Phos precatalyst in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 0.5 h; Inert atmosphere;
参考文献
Kinzel, Tom; Zhang, Yong; Buchwald, Stephen L.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14073 - 14075
