2-(6-氯吡啶-3-基)乙酸甲酯合成路线 (共 6 条)
参考文献
Leivers, Martin; Miller, John
Patent: US2011/52534 A1, 2011 ;
Location in patent: Page/Page column 90 ;
反应条件
in methanol; hexanes; ethyl acetate
参考文献
DOW AGROSCIENCES LLC
Patent: WO2004/57960 A2, 2004 ;
Location in patent: Page 13-14 ;
反应条件
sulfuric acid in 1,2-dichloro-ethane 5 h; Heating;
参考文献
Holla, B. Shivarama; Prasanna; Poojary, Boja; Rao; Shridhara; Bhat, U. Ganesha
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 864 - 868
反应条件
thionyl chloride in methanol
参考文献
US2014/142081 A1, ;
Page/Page column ;
反应条件
1: sulphuric acid / H2O / 3 h / Heating 2: 17.2 g / silphuric acid / 1,2-dichloro-ethane / 5 h / Heating View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 4 p. 864 - 868
反应条件
1: ethanol; H2O / 10 h / Heating 2: sulphuric acid / H2O / 3 h / Heating 3: 17.2 g / silphuric acid / 1,2-dichloro-ethane / 5 h / Heating View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 4 p. 864 - 868