反应条件
1: 1.) BuLi; 2.) t-BuOK / 1.) ether, hexane, from -60 deg C to 20 deg C; 2.) pentane, 3 h
2: CuBr / 1.) THF, -60 deg C; 2.) THF, 20 deg C, 2 h
3: 50 percent / acetylacetonate de vanadyle, peroxyde de tertiobutyle / benzene / 1 h at 20 deg C then 3 h at 50 deg C
View Scheme
参考文献
Douthreau, Alain; Sartoretti, Jacques; Gore, Jacques
Tetrahedron, 1983 , vol. 39, # 19 p. 3059 - 3066
