1,4-二氯-1,3-环己二烯合成路线 (共 1 条)
反应条件
1: 68.6 percent / 600 h / 100 °C
2: 64 percent / H2 / 5percent Pd on carbon / ethyl acetate / 12 h / 760 Torr
3: 84.8 percent / Al, I2 / CS2 / 1 h / 25 °C
4: 41.7 percent / di-n-butyltin dihydride, aqueous NaOH / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Wiseman, John R.; Vanderbilt, Jeffrey J.; Butler, William M.
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 667 - 671