N,N'-二甲基苯并咪唑鎓碘化物合成路线 （共 18 条）
反应条件
1: 16.3 percent / DMSO / nitrobenzene / 4 h / 130 - 160 °C
2: K2CO3 / H2O / Heating
View Scheme
参考文献
Glowczyk, Joanna; Serafin, Barbara
Polish Journal of Chemistry, 1984 , vol. 58, # 1-3 p. 149 - 156
反应条件
in acetonitrile
T=100°C; 0.166667 h; sealed flask;
参考文献
Khristich, B. I.; Bondarenko, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 284 - 287
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 339 - 342
反应条件
1: 71.6 percent / DMSO / 2 h / Heating
2: H2O / 1 h / Heating; other nucleophilic agents (methanol, sodium hydroxide); other 2-substituted 1,3-benzimidazolium iodides
View Scheme
参考文献
Glowczyk, Joanna; Serafin, Barbara
Polish Journal of Chemistry, 1984 , vol. 58, # 1-3 p. 149 - 156
反应条件
2: acetonitrile
View Scheme
参考文献
Kondo, Yasuhiko; Izawa, Shingo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1925 - 1928
反应条件
T=140 - 150°C; im Rohr;
参考文献
Fischer,O.; Rigaud
Chemische Berichte, 1902 , vol. 35, p. 1258
Show Details
Fischer,O.; Fussenegger
Chemische Berichte, 1901 , vol. 34, p. 936
反应条件
in tetrahydrofuran
11 h; Heating;
参考文献
Shi, Zhen; Gu, Huan
Synthetic Communications, 1996 , vol. 26, # 22 p. 4175 - 4179
反应条件
in tetrahydrofuran
11 h; Heating;
参考文献
Shi, Zhen; Gu, Huan
Synthetic Communications, 1996 , vol. 26, # 22 p. 4175 - 4179
反应条件
in tetrahydrofuran
11 h; Heating;
参考文献
Shi, Zhen; Gu, Huan
Synthetic Communications, 1996 , vol. 26, # 22 p. 4175 - 4179
