4-(2-溴苯基)-1-丁烯合成路线 (共 23 条)
反应条件
in tetrahydrofuran; diethyl ether 1.5 h; Heating;
参考文献
Molander, Gary A.; Sandrock, Deidre L.
Journal of the American Chemical Society, 2008 , vol. 130, # 47 p. 15792 - 15793
反应条件
magnesium in diethyl ether 20 h; Heating;
参考文献
Meijs,G.F.; Bunnett,J.F.; Beckwith,A.L.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4899
参考文献
Koppang,M.D.; Ross,G.A.; Woolsey,N.F.
Journal of the American Chemical Society, 1986 , vol. 108, p. 1441
反应条件
1: magnesium; allyl bromide in diethyl ether 2: 1-bromo-2-(bromomethyl)benzene in tetrahydrofuran
参考文献
Lin, Song; Song, Chun-Xiao; Cai, Gui-Xin; Wang, Wen-Hua; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, p. 12901 - 12903
反应条件
1.1: 9-borabicyclo[3.3.1]nonane / hexane / 18 h / 20 °C 1.2: 82 percent / NaOH; H2O2 / tetrahydrofuran / 1.5 h / 50 °C 2.1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C View Scheme
参考文献
Wolfe, John P.; Rennels, Roger A.; Buchwald, Stephen L.
Tetrahedron, 1996 , vol. 52, # 21 p. 7525 - 7546
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide direct-electrochemical reduction on Pt electrode; Epc = -2.80 V;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 1441
反应条件
potassium in ammonium hydroxide; tert-butyl alcohol Heating;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 4899
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=0 - 150°C;
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 464 - 465
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=20°C; 2.08333 h; Inert atmosphere;
参考文献
Hazimeh, Hassan; Mattalia, Jean-Marc; Marchi-Delapierre, Caroline; Kanoufi, Frederic; Combellas, Catherine; Chanon, Michel
European Journal of Organic Chemistry, 2009 , # 17 p. 2775 - 2787
反应条件
iodine; tert.-butyl lithium in diethyl ether; pentane T=-78°C;
参考文献
Bailey, William F.; Carson, Matthew W.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9960 - 9967