4-(2-溴苯基)-1-丁烯合成路线 （共 23 条）
反应条件
p-tert-butylbenzoic acid methyl ester; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Senboku, Hisanori; Michinishi, Jun-Ya; Hara, Shoji
Synlett, 2011 , # 11 p. 1567 - 1572
反应条件
1.1: 9-borabicyclo[3.3.1]nonane / hexane / 18 h / 20 °C
1.2: 82 percent / NaOH; H2O2 / tetrahydrofuran / 1.5 h / 50 °C
2.1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C
3.1: thionyl chloride / 0.75 h / Heating
View Scheme
参考文献
Wolfe, John P.; Rennels, Roger A.; Buchwald, Stephen L.
Tetrahedron, 1996 , vol. 52, # 21 p. 7525 - 7546
反应条件
p-tert-butylbenzoic acid methyl ester; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Senboku, Hisanori; Michinishi, Jun-Ya; Hara, Shoji
Synlett, 2011 , # 11 p. 1567 - 1572
