1-(4-(对甲苯氧基)苯基)乙酮合成路线 (共 9 条)
反应条件
tetrabutylammomium bromide; potassium carbonate in n-hexyl ether; dimethyl sulfoxide
T=130°C; Ullmann reaction; 12 h; Open air atmosphere;
参考文献
Islam, Manirul; Mondal, Sanchita; Mondal, Paramita; Roy, Anupam Singha; Hossain, Dildar; Mobarak, Manir
Transition Metal Chemistry, 2011 , vol. 36, # 1 p. 1 - 11
反应条件
copper (II) acetate monohydrate; caesium carbonate in N,N-dimethyl-formamide
T=100°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Chen, Jiuxi; Wang, Xingyong; Zheng, Xingwang; Ding, Jinchang; Liu, Miaochang; Wu, Huayue
Tetrahedron, 2012 , vol. 68, # 43 p. 8905 - 8907
反应条件
potassium phosphate; 2-((o-toluidino)methyl)phenol; copper(l) chloride in acetonitrile
T=81°C; Ullmann Condensation; 24 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
Qian, Cunwei; Qin, Liang; Zong, Qianshou; Wu, Lin; Fang, Dong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 12 p. 3915 - 3918
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=100°C;
参考文献
Cui, Sun-Liang; Jiang, Zhi-Yong; Wang, Yan-Guang
Synlett, 2004 , # 10 p. 1829 - 1831
反应条件
bis(μ-iodo)bis[(-)-sparteine]-dicopper(I); potassium carbonate in dimethyl sulfoxide
T=80°C; 12 h;
参考文献
Satyanarayana, Ponnam; Maheswaran, Hariharasarma; Kantam, Mannepalli Lakshmi; Bhargava, Suresh
Bulletin of the Chemical Society of Japan, 2011 , vol. 84, # 7 p. 788 - 790
反应条件
potassium phosphate in tetrahydrofuran
T=115°C; 18 h;
参考文献
Ghosh, Rajshekhar; Samuelson, Ashoka G.
New Journal of Chemistry, 2004 , vol. 28, # 11 p. 1390 - 1393
反应条件
potassium carbonate in N,N-dimethyl acetamide
Heating;
参考文献
Gorczynski, Michael J.; Leal, Rachel M.; Mooberry, Susan L.; Bushweller, John H.; Brown, Milton L.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 5 p. 1029 - 1036
反应条件
copper diacetate; copper
T=200°C;
参考文献
Horii; Kinouchi
Yakugaku Zasshi, 1937 , vol. 57, p. 683,688
Yakugaku Zasshi, 1938 , vol. 58, p. dtsch.Ref.S.293,295
Chem.Abstr., 1938 , p. 129
反应条件
carbon disulfide; aluminium trichloride
参考文献
Dilthey et al.
Journal fuer Praktische Chemie (Leipzig), 1927 , vol. <2>117, p. 359