反应条件
1: 2.) N-chlorosuccinimide, 3.) ethyldiisopropylamine / 1.) acetone, 2.) acetonitrile, -20 deg C, 5 min, 3.) acetonitrile, 80 deg C, 3 h
2: 56 percent / 170 - 180 °C / 0.01 Torr
3: 43 percent / LiAlH4 / diethyl ether / 24 h / Heating
View Scheme
参考文献
Altmeier, Peter; Vilsmaier, Elmar; Wolmershaeuser, Gotthelf
Tetrahedron, 1989 , vol. 45, # 10 p. 3189 - 3202
