4-(丁基氨基)苯甲酸甲酯合成路线 (共 7 条)
反应条件
2-(di-tert-butylphosphino)-2'-isopropoxy-1,1'-binaphthyl; caesium carbonate; palladium diacetate in ethylene glycol dimethyl ether
T=110°C; 16 h;
参考文献
Xie, Xiaomin; Zhang, Tony Y.; Zhang, Zhaoguo
Journal of Organic Chemistry, 2006 , vol. 71, # 17 p. 6522 - 6529
反应条件
palladium on activated charcoal in tetrahydrofuran
T=170°C; 1.5 h; Microwave irradiation;
参考文献
Linciano, Pasquale; Pizzetti, Marianna; Porcheddu, Andrea; Taddei, Maurizio
Synlett, 2013 , vol. 24, # 17 p. 2249 - 2254
反应条件
in tetrahydrofuran
T=20 - 25°C;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano; Ghigo, Giovanni
European Journal of Organic Chemistry, 2008 , # 5 p. 862 - 868
反应条件
in diethyl ether; hexane
T=-78 - 25°C; 0.833333 h;
参考文献
Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita
Synthesis, 2003 , # 5 p. 742 - 750
反应条件
acetic acid; zinc; benzene
参考文献
Surrey; Hammer
Journal of the American Chemical Society, 1944 , vol. 66, p. 2127
反应条件
sulfuric acid
Heating;
参考文献
Masunari, Andrea; Tavares, Leoberto Costa
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 12 p. 4229 - 4236
参考文献
Graf; Langer
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 148, p. 161,162