反应条件
1: 1) Mg / 1) THF, a) 0 to 5 deg C, 2 h, b) RT, overnight
2: 70 percent / mercuric acetate / 16 h / Heating
3: 5.7 g / 0.67 h / 160 - 165 °C
4: 1) NaH / 1) DMSO, 2) THF, RT, a) 2 h, b) overnight, 3) 50 to 55 deg C, 4 h
5: 90 percent / p-toluenesulphonic acid / methanol / 4 h
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Nanda, Rashmi; Puri, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 247 - 249
