1-(1,1-二甲基乙基)-3,5-二甲基-2,4-二硝基苯合成路线 (共 6 条)
反应条件
nitrogen(IV) oxide; ozone in hexane
T=-10°C; Nitration; 1.5 h;
参考文献
Suzuki, Hitomi; Hisatome, Kaori; Nonoyama, Nobuaki
Synthesis, 1999 , # 8 p. 1291 - 1293
反应条件
nitrogen(IV) oxide; ozone in dichloromethane
T=-10°C; Nitration; 3 h;
参考文献
Suzuki, Hitomi; Hisatome, Kaori; Nonoyama, Nobuaki
Synthesis, 1999 , # 8 p. 1291 - 1293
反应条件
methanesulfonic acid; nitrogen(IV) oxide; ozone in hexane
T=-10°C; Nitration; 1.5 h;
参考文献
Suzuki, Hitomi; Hisatome, Kaori; Nonoyama, Nobuaki
Synthesis, 1999 , # 8 p. 1291 - 1293
反应条件
sulfuric acid; nitric acid in dichloromethane
T=-10°C; Nitration; 9 h;
参考文献
Suzuki, Hitomi; Hisatome, Kaori; Nonoyama, Nobuaki
Synthesis, 1999 , # 8 p. 1291 - 1293
反应条件
cupric nitrate trihydrate supported on K 10 montmorillonite clay; nitric acid; acetic anhydride in tetrachloromethane
20 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Gigante, Barbara; Prazeres, Angela O.; Marcelo-Curto, Maria J.; Cornelis, Andre; Laszlo, Pierre
Journal of Organic Chemistry, 1995 , vol. 60, # 11 p. 3445 - 3447
反应条件
sulfuric acid; nitric acid
T=50 - 60°C;
参考文献
Baur
Chemische Berichte, 1900 , vol. 33, p. 2564