反应条件
1: 3,3-dimethyl-5-phenyldihydrofuran-2(3H)-one With diisobutylaluminium hydride in dichloromethane; toluene
T=-78°C; 2 h;
2: acetic anhydride With pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane; toluene
T=-78 - 22°C; 12 h;
参考文献
Smith, Deborah M.; Woerpel
Organic Letters, 2004 , vol. 6, # 12 p. 2063 - 2066