1: 60 percent / SiCl4 / ethanol / 24 h / 20 °C
2: 97 percent / CuI; Pd(PPh3)2Cl2; PPh3 / Et3N / tetrahydrofuran / 5 h / 20 °C
3: 85 percent / K2CO3 / methanol; tetrahydrofuran / 3 h / 20 °C
View Scheme
参考文献
Simpson, Christopher D.; Mattersteig, Gunter; Martin, Kai; Gherghel, Lileta; Bauer, Roland E.; Raeder, Hans Joachim; Muellen, Klaus
Journal of the American Chemical Society, 2004 , vol. 126, # 10 p. 3139 - 3147
1: 97 percent / CuI; Pd(PPh3)2Cl2; PPh3 / Et3N / tetrahydrofuran / 5 h / 20 °C
2: 85 percent / K2CO3 / methanol; tetrahydrofuran / 3 h / 20 °C
View Scheme
参考文献
Simpson, Christopher D.; Mattersteig, Gunter; Martin, Kai; Gherghel, Lileta; Bauer, Roland E.; Raeder, Hans Joachim; Muellen, Klaus
Journal of the American Chemical Society, 2004 , vol. 126, # 10 p. 3139 - 3147