2-溴甲基-3-甲氧基苯甲酸甲酯合成路线 （共 6 条）
反应条件
N-bromosuccinmide in tetrachloromethane 2 h; HeatingIrradiation;
参考文献
Boehringer Ingelheim (Canada) Ltd.
Patent: US2004/106791 A1, 2004 ;
Location in patent: Page 9 ;
反应条件
1: sulfuric acid / Inert atmosphere; Reflux 2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 1 h / Inert atmosphere; Reflux View Scheme
参考文献
European Journal of Inorganic Chemistry, , # 7 p. 1112 - 1120
反应条件
1: thionyl chloride / 6 h / Reflux 2: N-bromosuccinmide; 2-(4-biphenylyl)-5-phenyl-oxazole / tetrachloromethane / 80 °C View Scheme
参考文献
Chinese Chemical Letters, , vol. 23, # 1 p. 9 - 12
反应条件
methanol; ammonia 2 h; Reflux;
参考文献
Fu, Li Qiang; Ling, Chen Yu; Guo, Xing Sheng; He, Hui Li; Yang, Yu She
Chinese Chemical Letters, 2012 , vol. 23, # 1 p. 9 - 12
反应条件
1: methanol; ammonia / 2 h / Reflux
2: boron tribromide / 6 h / Reflux
View Scheme
参考文献
Fu, Li Qiang; Ling, Chen Yu; Guo, Xing Sheng; He, Hui Li; Yang, Yu She
Chinese Chemical Letters, 2012 , vol. 23, # 1 p. 9 - 12
反应条件
calcium carbonate in 1,4-dioxane; water
T=85°C; 3.5 - 4 h;
参考文献
Hormann, Robert Eugene; Potter, David W.; Chortyk, Orestes; Tice, Colin M.; Carlson, Glenn Richard; Meyer, Andrew; Opie, Thomas R.
Patent: US2006/20146 A1, 2006 ;
Location in patent: Page/Page column 32 ;
