2-((苯基硫代)甲基)吡啶合成路线 （共 11 条）
反应条件
TBA-Oxonereg; in dichloromethane 24 h; Ambient temperature;
参考文献
Trost, Barry M.; Braslau, Rebecca
Journal of Organic Chemistry, 1988 , vol. 53, # 3 p. 532 - 537
反应条件
caesium carbonate; cesium fluoride in N,N-dimethyl-formamide
T=20 - 60°C; Inert atmosphere;
参考文献
ALLA CHEM, LLC; Ivachtchenko, Alexandre Vasilievich; Mitkin, Oleg Dmitrievich; Kadieva, Madina Georgievna
Patent: US2013/267536 A1, 2013 ;
Location in patent: Paragraph 0176 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in benzene
24 h; Ambient temperature;
参考文献
Trost, Barry M.; Braslau, Rebecca
Journal of Organic Chemistry, 1988 , vol. 53, # 3 p. 532 - 537
反应条件
1: 2-picoline With n-butyllithium in hexane
2: diphenyldisulfane in hexane
参考文献
Jones, Roderick C.; Canty, Allan J.; Gardiner, Michael G.; Skelton, Brian W.; Tolhurst, Vicki-Anne; White, Allan H.
Inorganica Chimica Acta, 2010 , vol. 363, # 1 p. 77 - 87
反应条件
1: sodium tetrahydroborate; sodium hydroxide / ethanol / |Inert atmosphere
2: ethanol / |Inert atmosphere
View Scheme
参考文献
Prakash, Om; Sharma, Kamal Nayan; Joshi, Hemant; Gupta, Pancham Lal; Singh, Ajai K.
Dalton Transactions, 2013 , vol. 42, # 24 p. 8736 - 8747
反应条件
hydrogen bromide
24 h; Heating;
参考文献
Haviv, Fortuna; DeNet, Robert W.; Michaels, Raymond J.; Ratajczyk, James D.; Carter, George W.; Young, Patrick R.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 2 p. 218 - 222
反应条件
in acetone
2 h; Ambient temperature;
参考文献
Mentz; Modro
Canadian Journal of Chemistry, 1994 , vol. 72, # 9 p. 1933 - 1960
反应条件
triethylamine in methanol
T=60°C; Rate constant;
参考文献
Terashima, Isamu; Kohda, Kohfuku
Journal of Medicinal Chemistry, 1998 , vol. 41, # 4 p. 503 - 508
反应条件
triethylamine in methanol
T=60°C; dealkylation; Kinetics;
参考文献
Kohda; Terashima; Koyama; Watanabe; Mineura
Biological and Pharmaceutical Bulletin, 1995 , vol. 18, # 3 p. 424 - 430
反应条件
in ethanol
Inert atmosphere;
参考文献
Prakash, Om; Sharma, Kamal Nayan; Joshi, Hemant; Gupta, Pancham Lal; Singh, Ajai K.
Dalton Transactions, 2013 , vol. 42, # 24 p. 8736 - 8747
