1: acridone acid With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0 - 60°C; 2: methyl iodide in N,N-dimethyl-formamide; mineral oil T=60°C; 18 h;
oxygen; methylene blue in dichloromethane T=-78°C; 0.05 h; Irradiation;
参考文献
Suzuki, Nobutaka; Sano, Kaniti; Wakatsuki, Satoshi; Tani, Noriyuki; Izawa, Yasuji
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 10 p. 3351 - 3352
1: With cesium fluoride in acetonitrile T=65°C; 10 h; 2: With hydrogenchloride in acetonitrile T=65°C; 4 h; 3: With water; sodium methylate in acetonitrile T=100°C; 2 h;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Organic Letters, 2011 , vol. 13, # 15 p. 4136 - 4139
1: With cesium fluoride in acetonitrile T=65°C; 10 h; 2: With hydrogenchloride in acetonitrile T=65 - 100°C; 4 h; 3: With water in acetonitrile T=100°C; 2 h;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Organic Letters, 2011 , vol. 13, # 15 p. 4136 - 4139