1,2,4-噻唑[4,3-b]吡嗪e, 6-氯-3-苯基-合成路线 （共 12 条）
反应条件
1: hydrazine hydrate / ethanol / 1 h / 60 °C / |Inert atmosphere
2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium carbonate / toluene / 100 °C / |Inert atmosphere
3: chloroamine-T trihydrate / 2-methyl tetrahydrofuran / 2 h / 60 °C / |Inert atmosphere
View Scheme
参考文献
Thiel, Oliver R.; Achmatowicz, Michal M.
Organic Syntheses, 2013 , vol. 90, p. 287 - 300
反应条件
1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium carbonate / toluene / 100 °C / |Inert atmosphere
2: chloroamine-T trihydrate / 2-methyl tetrahydrofuran / 2 h / 60 °C / |Inert atmosphere
View Scheme
参考文献
Thiel, Oliver R.; Achmatowicz, Michal M.
Organic Syntheses, 2013 , vol. 90, p. 287 - 300
