1-(2-羟基-5-碘-苯基)-乙酮合成路线 （共 6 条）
反应条件
1: With sulfuric acid; sodium nitrite in water
0.583333 h;
2: With sulfuric acid; copper; potassium iodide in water
T=20 - 65°C;
参考文献
ROWETT RESEARCH INSTITUTE
Patent: WO2004/7475 A1, 2004 ;
Location in patent: Page 74-75 ;
反应条件
NH4I; Oxonereg; in methanol
2.3 h; Reflux; regioselective reaction;
参考文献
Marri, Mahender Reddy; MacHarla, Arun Kumar; Peraka, Swamy; Nama, Narender
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6554 - 6559
反应条件
N-iodo-succinimide; toluene-4-sulfonic acid in acetonitrile
T=20°C; 14 h; regioselective reaction;
参考文献
Bovonsombat, Pakorn; Leykajarakul, Juthamard; Khan, Chiraphorn; Pla-on, Kawin; Krause, Michael M.; Khanthapura, Pratheep; Ali, Rameez; Doowa, Niran
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2664 - 2667
参考文献
Covello; Piscopo
Gazzetta Chimica Italiana, 1958 , vol. 88, p. 101,108
反应条件
aluminium trichloride; nitrobenzene
参考文献
Chen; Chang
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1954 , vol. <II>1, p. 156
反应条件
aluminium trichloride; nitrobenzene
参考文献
Chen; Chang
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1954 , vol. <II>1, p. 156
