N-(2-溴苯基)肉桂酰胺合成路线 （共 5 条）
反应条件
1: With AlCl3, aluminium chloride in chlorobenzene T=125°C; 2 h; 2: With water in chlorobenzene T=0°C;
参考文献
Cailleau, Nathalie; Davies, David Thomas; Esken, Joel Michael; Hennessy, Alan Joseph; Kusalakumari Sukumar, Senthil Kumar; Markwell, Roger Edward; Miles, Timothy James; Pearson, Neil David
Patent: US2008/221110 A1, 2008 ;
Location in patent: Page/Page column 38 ;
反应条件
1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 125 °C 2: trichlorophosphate / 2 h / 125 °C 3: methanol / 5 h / Reflux View Scheme
参考文献
Ullah, Nisar
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 1 p. 75 - 84
反应条件
1: 56 percent / aluminium chloride / chlorobenzene / 2 h / 125 °C 2: 83 percent / phosphorus oxychloride / 2 h / 125 °C View Scheme
参考文献
Ullah, Nisar
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 1 p. 75 - 84
反应条件
1: 56 percent / aluminium chloride / chlorobenzene / 2 h / 125 °C
2: 83 percent / phosphorus oxychloride / 2 h / 125 °C
3: 79 percent / diisopropylamine; butyllithium; iodine / tetrahydrofuran; hexane / 2 h / -75 °C
View Scheme
参考文献
Cottet, Fabrice; Marull, Marc; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2003 , # 8 p. 1559 - 1568
反应条件
1: 56 percent / aluminium chloride / chlorobenzene / 2 h / 125 °C
2: 83 percent / phosphorus oxychloride / 2 h / 125 °C
3: 79 percent / diisopropylamine; butyllithium; iodine / tetrahydrofuran; hexane / 2 h / -75 °C
4: 64 percent / copper iodide; potassium fluoride / 1-methyl-pyrrolidin-2-one / 20 h / 50 °C
View Scheme
参考文献
Cottet, Fabrice; Marull, Marc; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2003 , # 8 p. 1559 - 1568
