3H-螺(1-苯并呋喃-2,3-吡咯烷)合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated charcoal in isopropyl alcohol
T=50°C; P=2430.6 Torr;
参考文献
Effland, Richard C.; Gardner, Beth Ann; Strupczewski, Joseph
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 811 - 814
反应条件
1: 70 percent / 98percent sodium hydride / benzene; dimethylformamide / 120 h / 90 °C
2: 75 percent / H2 / 10percent palladium on charcoal / propan-2-ol / 50 °C / 2430.6 Torr
View Scheme
参考文献
Effland, Richard C.; Gardner, Beth Ann; Strupczewski, Joseph
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 811 - 814
反应条件
1: 1.) magnesium / 1.) iodine / 1.) ether, reflux, 20 h; 2.) ether, r.t., 2 h
2: 70 percent / 98percent sodium hydride / benzene; dimethylformamide / 120 h / 90 °C
3: 75 percent / H2 / 10percent palladium on charcoal / propan-2-ol / 50 °C / 2430.6 Torr
View Scheme
参考文献
Effland, Richard C.; Gardner, Beth Ann; Strupczewski, Joseph
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 811 - 814
