sodium hydride in DMF (N,N-dimethyl-formamide)
T=-5 - 20°C; 2.5 h;
参考文献
Waddell, Sherman T.; Santorelli, Gina M.; Maletic, Milana M.; Leeman, Aaron H.; Gu, Xin; Graham, Donald W.; Balkovec, James M.; Aster, Susan D.
Patent: US2004/133011 A1, 2004 ;
Location in patent: Page 19-20 ;
potassium tert-butylate in tetrahydrofuran
T=0 - 40°C; 5 h;
参考文献
Barber, Christopher Gordon; Bunnage, Mark Edward; Harvey, John Wilson; Mathias, John Paul
Patent: US2005/20611 A1, 2005 ;
Location in patent: Page/Page column 39 ;
sodium hydroxide; water in ethanol
60 h; Heating / reflux;
参考文献
Barber, Christopher Gordon; Bunnage, Mark Edward; Harvey, John Wilson; Mathias, John Paul
Patent: US2005/20611 A1, 2005 ;
Location in patent: Page/Page column 40 ;
