2-{[(4-氯苯基)氨基]甲基}苯酚合成路线 (共 7 条)
反应条件
sodium tetrahydroborate in methanol
0.5 h; Ambient temperature;
参考文献
Joglekar, S. J.; Samant, S. D.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 110 - 111
反应条件
1: ethanol / 3 h / Reflux
2: sodium tetrahydroborate / methanol / 0.67 h / 0 °C
View Scheme
参考文献
Tang, Zilong; Chen, Weiwen; Zhu, Zhonghua; Liu, Hanwen
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 2 p. 255 - 260
反应条件
1: ethanol / 3 h / Reflux
2: sodium tetrahydroborate / methanol / 0.67 h / 0 °C
View Scheme
参考文献
Tang, Zilong; Chen, Weiwen; Zhu, Zhonghua; Liu, Hanwen
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 2 p. 255 - 260
反应条件
triethylamine in dichloromethane
8 h; Ambient temperature;
参考文献
Mayadeo, M. S.; Kulkarni, S. J.; Deodhar, K. D.
Synthesis, 1990 , # 1 p. 87 - 88
反应条件
ethanol
T=150°C; im Druckrohr;
参考文献
Paal
Archiv der Pharmazie (Weinheim, Germany), 1902 , vol. 240, p. 689
反应条件
(i), (ii) NaBH4; Multistep reaction;
参考文献
Derieg,M.E.; Sternbach,L.H.
Journal of Heterocyclic Chemistry, 1966 , vol. 3, p. 237 - 238
反应条件
in benzene
byproducts: H2; 9-BBN added to benzene soln. of nitrone of salicyl aldehyde, warmed to 50°C for some min; added petroleum ether, recrystd. from methanol, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386