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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
71965-05-4
合成路线
（共 7 条）
71965-05-4
+
50-00-0
甲醛
→
反应条件
343603-91-8
反应条件
1: 3-(2'-methylphenyl)phenol With methylmagnesium bromide in tetrahydrofuran; diethyl ether T=0°C; 0.5 h; 2: formaldehyd With triethylamine in benzene 24 h; Reflux;
参考文献
Chinigo, Gary M.; Paige, Mikell; Grindrod, Scott; Hamel, Ernest; Dakshanamurthy, Sivanesan; Chruszcz, Maksymilian; Minor, Wladek; Brown, Milton L.
Journal of Medicinal Chemistry, 2008 , vol. 51, # 15 p. 4620 - 4631
854726-99-1
→
反应条件
71965-05-4
反应条件
hydrogen bromide; oxygen; copper(ll) bromide in 1,4-dioxane; water T=20°C; 20 h; Sealed tube;
参考文献
Kikushima, Kotaro; Nishina, Yuta
RSC Advances, 2013 , vol. 3, # 43 p. 20150 - 20156
878996-36-2
→
反应条件
71965-05-4
反应条件
1: With boron tribromide in dichloromethane T=20°C; 5 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran 1 h; Heating;
参考文献
Shi, Yijian; Wan, Peter
Canadian Journal of Chemistry, 2005 , vol. 83, # 9 p. 1306 - 1323
135227-03-1
→
反应条件
71965-05-4
反应条件
boron tribromide in dichloromethane T=0 - 20°C; Kumada coupling reaction; Inert atmosphere;
参考文献
Jin, Zhong; Li, Yan-Jing; Ma, Yong-Qiang; Qiu, Ling-Ling; Fang, Jian-Xin
Chemistry - A European Journal, 2012 , vol. 18, # 2 p. 446 - 450
932-31-0
邻甲苯基溴化镁
→
反应条件
71965-05-4
反应条件
1: NiII chloride hexahydrate; C32H39N2OP / tetrahydrofuran / 20 h / 25 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Jin, Zhong; Li, Yan-Jing; Ma, Yong-Qiang; Qiu, Ling-Ling; Fang, Jian-Xin
Chemistry - A European Journal, 2012 , vol. 18, # 2 p. 446 - 450
2845-89-8
3-氯苯甲醚
→
反应条件
71965-05-4
反应条件
1: NiII chloride hexahydrate; C32H39N2OP / tetrahydrofuran / 20 h / 25 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Jin, Zhong; Li, Yan-Jing; Ma, Yong-Qiang; Qiu, Ling-Ling; Fang, Jian-Xin
Chemistry - A European Journal, 2012 , vol. 18, # 2 p. 446 - 450
16419-60-6
2-甲基苯硼酸
→
反应条件
71965-05-4
反应条件
1: [Pd(CH3CN)4](BF4)2; 6,6'-dimethyl-2,2'-bipyridine; anthraquinone-2-sulfonic acid sodium salt; oxygen / 1-methyl-pyrrolidin-2-one / 13 h / 50 °C / 760.05 Torr 2: dimethyl sulfoxide; 1-methyl-pyrrolidin-2-one / 36 h / 80 °C View Scheme
参考文献
Izawa, Yusuke; Zheng, Changwu; Stahl, Shannon S.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 13 p. 3672 - 3675
Angew. Chem., 2013 , vol. 125, # 13 p. 3760 - 3763,4
