N-bromosuccinmide; potassium carbonate in ethanol; water
T=0 - 5°C; 1 h;
参考文献
Hansen, John F.; Kim, Yong In; Griswold, Linus J.; Hoelle, Gary W.; Taylor, Deborah L.; Vietti, David E.
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 76 - 80
1: 97 percent / NH2OH*HCl, aq. HCl / ethanol / 15 h / 5 °C
2: 96 percent / 1.) butyl nitrite, pyridine, copper(II) sulphate pentahydrate, 2.) 5percent aq. KOH / aq. ethanol / other (E)- and (Z)-oximes
View Scheme
参考文献
Hansen, John F.; Easter, John A.; Eckert, David A.; Hunt, Karen J.; Little, David A.
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 2 p. 281 - 286