1: (1,1,1-tributylstannyl)benzene; 9-anthracenemethyl-4-bromobenzoate With tetrakis(triphenylphosphine) palladium(0) in toluene T=100°C; Stille coupling; 12 h; 2: With N-benzylmaleimide resin in toluene T=90°C; 8 h; 3: methanol With sodium methylate in tetrahydrofuran 0.5 h; Further stages.;
参考文献
Wang; Parlow; Porco Jr.
Organic letters, 2000 , vol. 2, # 22 p. 3509 - 3512