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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7204-23-1
合成路线
（共 10 条）
1040171-12-7
→
反应条件
7204-23-1
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=0°C; 0.05 h;
参考文献
Hayakawa, Ichiro; Watanabe, Hidekazu; Kigoshi, Hideo
Tetrahedron, 2008 , vol. 64, # 25 p. 5873 - 5877
1040170-94-2
→
反应条件
7204-23-1
反应条件
hydrogenchloride in tetrahydrofuran; methanol T=100°C;
参考文献
Hayakawa, Ichiro; Watanabe, Hidekazu; Kigoshi, Hideo
Tetrahedron, 2008 , vol. 64, # 25 p. 5873 - 5877
1040170-94-2
→
反应条件
7204-23-1
+
1040171-01-4
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=-20°C; 0.0833333 h;
参考文献
Hayakawa, Ichiro; Watanabe, Hidekazu; Kigoshi, Hideo
Tetrahedron, 2008 , vol. 64, # 25 p. 5873 - 5877
946489-39-0
→
反应条件
7204-23-1
反应条件
Fremy’s salt in water; acetone T=20°C; 3 h;
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
946489-38-9
→
反应条件
7204-23-1
反应条件
1: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 2: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
844-51-9
2,5-二苯基-对-苯醌
→
反应条件
7204-23-1
反应条件
1: 73 percent / aq. perchloric acid / 2 h / 70 °C 2: 90 percent / K2CO3 / methanol / 3 h / 0 °C 3: 84 percent / K2CO3 / dimethylformamide / 5 h / 20 °C 4: aq. HCl / dioxane / 24 h / 80 °C 5: 1.86 g / K2CO3 / dimethylformamide / 1 h / 60 °C 6: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 7: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
20955-74-2
→
反应条件
7204-23-1
反应条件
1: 90 percent / K2CO3 / methanol / 3 h / 0 °C 2: 84 percent / K2CO3 / dimethylformamide / 5 h / 20 °C 3: aq. HCl / dioxane / 24 h / 80 °C 4: 1.86 g / K2CO3 / dimethylformamide / 1 h / 60 °C 5: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 6: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
803725-38-4
→
反应条件
7204-23-1
反应条件
1: 84 percent / K2CO3 / dimethylformamide / 5 h / 20 °C 2: aq. HCl / dioxane / 24 h / 80 °C 3: 1.86 g / K2CO3 / dimethylformamide / 1 h / 60 °C 4: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 5: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
803725-40-8
→
反应条件
7204-23-1
反应条件
1: 1.86 g / K2CO3 / dimethylformamide / 1 h / 60 °C 2: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 3: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
803725-39-5
→
反应条件
7204-23-1
反应条件
1: aq. HCl / dioxane / 24 h / 80 °C 2: 1.86 g / K2CO3 / dimethylformamide / 1 h / 60 °C 3: hydrogen / Pd/C / ethyl acetate; ethanol / 5 h / 20 °C / 760 Torr 4: 1.11 g / potassium nitrosodisulfonate / H2O; acetone / 3 h / 20 °C View Scheme
参考文献
Sawayama, Yusuke; Tsujimoto, Takashi; Sugino, Kumi; Nishikawa, Toshio; Isobe, Minoru; Kawagishi, Hirokazu
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 12 p. 2998 - 3003
