1-(异丙基硫代)-4-硝基苯合成路线 （共 13 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide
12 h;
参考文献
Branstetter, Bryan James; Breitenbucher, James Guy; Lebsack, Alec D.; Xiao, Wei
Patent: US2008/4253 A1, 2008 ;
Location in patent: Page/Page column 14-15 ;
US 20080004253 A1
反应条件
in N,N-dimethyl-formamide
T=90°C;
参考文献
PALAU PHARMA, S.A.; SALAS SOLANA, Jorge; ALMANSA ROSALES, Carmen; SOLIVA SOLIVA, Robert; FONTES USTRELL, Montserrat; COMELLES ESPUGA, Josep
Patent: WO2010/34740 A1, 2010 ;
Location in patent: Page/Page column 70-71 ;
WO 2010/034740 A1
反应条件
cesium fluoride in acetonitrile
T=82°C;
参考文献
Shah, Syed Tasadaque Ali; Khan, Khalid Mohammed; Martinez Heinrich, Angelica; Voelter, Wolfgang
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8281 - 8283
Title/Abstract View citing articles Show Details
Shah, Syed T. A.; Khan, Khalid M.; Hussain, Hidayat; Hayat, Safdar; Voelter, Wolfgang
Monatshefte fur Chemie, 2005 , vol. 136, # 9 p. 1583 - 1589
反应条件
1: 1-chloro-4-nitro-benzene With palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=20°C; 0.0833333 h; Inert atmosphere;
2: (i-PrS)3In With caesium carbonate in N,N-dimethyl-formamide
T=100°C; 3 h; Inert atmosphere;
参考文献
Atobe, Shingo; Sonoda, Motohiro; Suzuki, Yuki; Shinohara, Hiroyuki; Yamamoto, Takuya; Ogawa, Akiya
Chemistry Letters, 2011 , vol. 40, # 9 p. 980 - 982
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.333333 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
potassium carbonate in dichloromethane
96 h; Ambient temperature;
参考文献
Umemura, Kazuyuki; Matsuyama, Haruo; Kamigata, Nobumasa
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, p. 2593 - 2600
反应条件
in ethanol
12 h; Ambient temperature;
参考文献
Pasto, Daniel J.; Cottard, Francois; Jumelle, Laurent
Journal of the American Chemical Society, 1994 , vol. 116, # 20 p. 8978 - 8984
反应条件
potassium hydroxide in ethanol; water
Ice coolingRefluxInert atmosphere;
参考文献
Hanson, Peter; Hendrickx, Ramon A. A. J.; Lindsay Smith, John R.
New Journal of Chemistry, 2010 , vol. 34, # 1 p. 65 - 84
反应条件
in isopropyl alcohol
T=40°C; Product distributionKineticsMechanism;
参考文献
Montanari, Stefano; Paradisi, Cristina; Scorrano, Gianfranco
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4274 - 4279
参考文献
Flowers,W.T. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2394 - 2398
