N-苄氧羰基乙二胺盐酸盐合成路线 （共 17 条）
反应条件
1: With potassium acetate in ethylene glycol dimethyl ether; ethanol; water T=20°C; 1 h; 2: With water; sodium hydroxide
参考文献
Milne, Jill C.; Jirousek, Michael R.; Bemis, Jean E.; Smith, Jesse J.
Patent: US2010/41748 A1, 2010 ;
Location in patent: Page/Page column 115 ;
反应条件
in dichloromethane T=0 - 20°C; 25 h;
参考文献
Squire, Jennifer S.; Sutti, Alessandra; Durand, Gregory; Conlan, Xavier A.; Henderson, Luke C.
New Journal of Chemistry, 2013 , vol. 37, # 7 p. 1895 - 1905
反应条件
in chloroform; water 1 h;
参考文献
Mpex Pharmaceuticals, Inc.
Patent: US2008/318957 A1, 2008 ;
Location in patent: Page/Page column 57; 58 ;
反应条件
sodium hydroxide; ethylenediamine in methanol; water
参考文献
Ponticello; Ignazio S.; Hollister; Kenneth R.; Tuites; Richard C.
Patent: US4346231 A1, 1982 ;
反应条件
triphenylphosphine in methanol; water 2 h; Reflux;
参考文献
Park, Jin-Hun; Oh, Chang-Hyun
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 2854 - 2860
参考文献
Pittelkow, Michael; Lewinsky, Rasmus; Christensen, Jorn Bolstad
Synthesis, 2002 , # 15 p. 2195 - 2202
反应条件
1: 88 percent / triethylamine / CH2Cl2 / 1.) 0 deg C, 30 min, 2.) RT, 30 min 2: 93 percent / sodium azide / hexamethylphosphoric acid triamide / 6 h / 55 °C 3: sodium borohydride / 10percent palladium on charcoal / H2O; methanol / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3117 - 3132
反应条件
1: 93 percent / sodium azide / hexamethylphosphoric acid triamide / 6 h / 55 °C 2: sodium borohydride / 10percent palladium on charcoal / H2O; methanol / Ambient temperature View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3117 - 3132
反应条件
pyridine; bis-[(trifluoroacetoxy)iodo]benzene in water; N,N-dimethyl-formamide T=0 - 20°C; Hofmann reaction; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 3 p. 699 - 709
反应条件
hydrogenchloride in acetic acid
参考文献
Hoppe-Seyler's Zeitschrift fuer physiologische Chemie, , vol. 349, # 2 p. 251 - 262
