N-苄氧羰基乙二胺盐酸盐合成路线 (共 17 条)
反应条件
1: pyridine / dichloromethane / 16 h / 20 °C / |Inert atmosphere 2: ethanol / 16 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 17 p. 2675 - 2685
反应条件
1: triethylamine / dichloromethane / 1.5 h / 0 °C 2: triethylamine / dichloromethane / 1.5 h / 0 °C 3: sodium azide / dimethyl sulfoxide / 2 h / 70 °C 4: triphenylphosphine / methanol; water / 2 h / Reflux View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 12 p. 5769 - 5777
反应条件
1: tributylamine / tetrahydrofuran / 0.17 h / -20 °C 2: 152 mg / aq. NH3 / tetrahydrofuran / 1 h / 0 °C 3: pyridine; [bis(trifluoroacetoxy)iodo]benzene / dimethylformamide; H2O / 3 h / 0 - 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 3 p. 699 - 709
反应条件
dimethylsulfide borane complex in tetrahydrofuran; dichloromethane 24.3333 h; RefluxInert atmosphere;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 2 p. 248 - 254
参考文献
DE676049 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 25, p. 495
反应条件
hydrogen; palladium on activated charcoal in methanol 4 h;
参考文献
Kokotos, George; Constantinou-Kokotou, Violetta
Journal of Chemical Research, Miniprint, 1992 , # 12 p. 3117 - 3132
反应条件
in acetone 1.) room temp., 24 h, 2.) reflux, 1 h;
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465