Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
1: 85 percent / diethyl ether / 1 h
2: 76 percent / NaOEt / 0.5 h / Ambient temperature
3: 92 percent / KOH / dimethylsulfoxide / 1 h
4: 65 percent / 70percent HNO3 / 1 h / 30 °C
5: 2 M aq. HCl / Heating
View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
1: 92 percent / KOH / dimethylsulfoxide / 1 h
2: 65 percent / 70percent HNO3 / 1 h / 30 °C
3: 2 M aq. HCl / Heating
View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
1: 76 percent / NaOEt / 0.5 h / Ambient temperature
2: 92 percent / KOH / dimethylsulfoxide / 1 h
3: 65 percent / 70percent HNO3 / 1 h / 30 °C
4: 2 M aq. HCl / Heating
View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
potassium tert-butylate in dimethyl sulfoxide
2 h; Ambient temperature;
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
1: 65 percent / 70percent HNO3 / 1 h / 30 °C
2: 2 M aq. HCl / Heating
View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
nitric acid; acetic anhydride
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Skvortsov, I. M.; Astakhova, L. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 11 p. 1189 - 1191
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 11 p. 1489 - 1491
