N-(2-氨基苯基)苯甲酰胺合成路线 （共 30 条）
反应条件
copper(I) oxide; water; caesium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate; sodium hydroxide; N-methyl-2-(methylamino)ethylamine
T=100°C; 16 h; Inert atmosphereSealed tube;
参考文献
Wang, Jichao; Yin, Xinchi; Wu, Jun; Wu, Datong; Pan, Yuanjiang
Tetrahedron, 2013 , vol. 69, # 48 p. 10463 - 10469
反应条件
sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate
T=120°C; 12 h;
参考文献
Liang, Jun; Lv, Jing; Shang, Zhi-Cai
Tetrahedron, 2011 , vol. 67, # 44 p. 8532 - 8535
反应条件
copper(l) iodide; ammonia; caesium carbonate; L-proline in water; dimethyl sulfoxide
T=20°C; Inert atmosphere;
参考文献
Diao, Xiaoqiong; Wang, Yuji; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7974 - 7977
反应条件
triethylamine in dichloromethane
2 h; Inert atmosphereReflux;
参考文献
Suhonen, Aku; Nauha, Elisa; Salorinne, Kirsi; Helttunen, Kaisa; Nissinen, Maija
CrystEngComm, 2012 , vol. 14, # 21 p. 7398 - 7407,10
反应条件
K3PO4*3H2O; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 10 h; Inert atmosphere;
参考文献
Yao, Zijian; Wei, Xianwen
Chinese Journal of Chemistry, 2010 , vol. 28, # 11 p. 2260 - 2268
反应条件
1: 97 percent / pyridine / 15 h / 25 °C
2: 80 percent / H2 / 5 percent Pd/C / methanol / 15 h
View Scheme
参考文献
Kaiya; Fujiwara; Kohda
Chemical Research in Toxicology, 2000 , vol. 13, # 10 p. 993 - 1001
反应条件
1: 1,2-diamino-benzene With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
2: benzaldehyde With YCl3 in toluene
T=20°C; Cannizzaro reaction; 48 h; Inert atmosphere;
3: With hydrogenchloride in water; toluene
T=20°C; Inert atmosphere;
参考文献
Zhang, Lijun; Su, Shunpeng; Wu, Hongping; Wang, Shaowu
Tetrahedron, 2009 , vol. 65, # 48 p. 10022 - 10024
反应条件
in water
T=80°C; 16 h; Sealed tube;
参考文献
Hikawa, Hidemasa; Imani, Maki; Suzuki, Hideharu; Yokoyama, Yuusaku; Azumaya, Isao
RSC Advances, 2014 , vol. 4, # 8 p. 3768 - 3773
反应条件
1: 97 percent / pyridine / 15 h / 25 °C
2: 80 percent / H2 / 5 percent Pd/C / methanol / 15 h
View Scheme
参考文献
Kaiya; Fujiwara; Kohda
Chemical Research in Toxicology, 2000 , vol. 13, # 10 p. 993 - 1001
反应条件
copper(l) iodide; sodium azide; ethanol; potassium carbonate; N-methyl-2-(methylamino)ethylamine
T=20 - 78°C; Inert atmosphereSealed tube;
参考文献
Zhao, Haibo; Fu, Hua; Qiao, Renzhong
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3311 - 3316
