4-(三氟甲基)苯乙酸乙酯合成路线 （共 10 条）
反应条件
4-(N,N-dimethlyamino)pyridine; bis(η3-allyl-μ-chloropalladium(II)); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,3,5-trimethyl-benzene T=140°C; 20 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 9 p. 2113 - 2120
反应条件
4-(N,N-dimethlyamino)pyridine; bis(η3-allyl-μ-chloropalladium(II)); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,3,5-trimethyl-benzene T=140°C; 20 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 9 p. 2113 - 2120
反应条件
sulfuric acid 48 h; Heating / reflux;
参考文献
WO2008/76427 A2, ;
Page/Page column 66 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); i-Pr2NPPh2; water; potassium carbonate in tetrahydrofuran T=65°C; 8 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 66, # 42 p. 8238 - 8241
反应条件
potassium carbonate; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 T=160°C; 8 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 9 p. 1565 - 1574
反应条件
potassium carbonate; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 T=160°C; 8 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 9 p. 1565 - 1574
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide Ambient temperatureelectrolysis, reticulated vitreous carbon cathode;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2732 - 2754
反应条件
hydrogenchloride; potassium hydroxide; copper(l) iodide in 1,4-dioxane 114 h; Heating;
参考文献
Journal of Fluorine Chemistry, , vol. 40, p. 81 - 98
参考文献
Journal of Organic Chemistry, , vol. 74, # 6 p. 2571 - 2574
