2-(2,6-二甲基苯氧基)乙醛合成路线 （共 4 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide in dichloromethane
T=-78 - 0°C; 1.66667 h;
参考文献
NEUROTECH CO., LTD.
Patent: WO2007/119984 A1, 2007 ;
Location in patent: Page/Page column 44-45 ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide
2: sulfuric acid
View Scheme
参考文献
Oezdemir, Ahmet; Turan-Zitouni, Guelhan; Kaplancikli, Zafer Asim; Altintop, Mehlika Dilek
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 2 p. 141 - 146
反应条件
dimethylsulfide; ozone
1.) CH2Cl2, MeOH, -40 deg C, 2.) -40 deg C to room temp.; Yield given. Multistep reaction;
参考文献
Jellen; Mittelbach; Junek
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 167 - 172
参考文献
Oezdemir, Ahmet; Turan-Zitouni, Guelhan; Kaplancikli, Zafer Asim; Altintop, Mehlika Dilek
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 2 p. 141 - 146
