N-Boc-L-苯丙氨醛合成路线 （共 60 条）
反应条件
hydrogenchloride in diethyl ether
反应条件
Li(Et3CO)3AlH in tetrahydrofuran T=0°C;
参考文献
Tetrahedron Letters, , vol. 35, # 48 p. 9031 - 9034
反应条件
lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=-75 - -70°C; 0.166667 h;
参考文献
Tetrahedron Letters, , vol. 36, # 40 p. 7281 - 7284
反应条件
lithium borohydride in tetrahydrofuran
反应条件
1: 98 percent / aq. NaHCO3 / dioxane / 12 h / 20 °C 2: 80 percent / DIBAL-H / CH2Cl2; hexane / 2 h / -78 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 36 p. 7877 - 7883
反应条件
1: Et3N; DMAP / CH2Cl2 / 2 h / 20 °C 2: 81 percent / H2 / Pd/C / methanol / 2 h / 20 °C View Scheme
参考文献
Organic letters, , vol. 3, # 6 p. 897 - 899
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran Reduction; 0.25 h; 2: With potassium hydrogensulfate Hydrolysis;
参考文献
Tetrahedron Letters, , vol. 41, # 1 p. 37 - 40
反应条件
tert.-butylnitrite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; boron trifluoride diethyl etherate in dichloromethane 24 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 16, # 1 p. 58 - 61
反应条件
diisobutylaluminium hydride in dichloromethane T=-78°C;
参考文献
Synlett, , # 3 p. 435 - 439
反应条件
silver nitrate in water; acetonitrile T=20°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 23 p. 9522 - 9524
