1: 2-methylindan-1-one With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: methoxycarbonyl cyanide in tetrahydrofuran
T=-78 - -20°C; 0.666667 h;
参考文献
Barvian, Kevin Karl; Speake, Jason Daniel; Cowan, David John; Larkin, Andrew Lamont; Szewczyk, Jerzy Ryszard
Patent: US2009/54431 A1, 2009 ;
Location in patent: Page/Page column 44-45 ;
