1,17-二氨基-3,6,9,12,15-五氧杂十七烷合成路线 （共 6 条）
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 24 h;
参考文献
LaFrate, Andrew L.; Carlson, Kathryn E.; Katzenellenbogen, John A.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 10 p. 3528 - 3535
反应条件
sodium carbonate in water
反应条件
ammonium hydroxide; sodium carbonate in water
反应条件
1: 90 percent / aq. NaOH / tetrahydrofuran / 3 h / 0 °C 2: NaN3 / dimethylformamide / 8 h / 100 °C 3: H2 / ethanol; ethyl acetate / 5 h / 20 °C / 2844.31 Torr View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 34 p. 5441 - 5447
反应条件
1: NaN3 / dimethylformamide / 8 h / 100 °C 2: H2 / ethanol; ethyl acetate / 5 h / 20 °C / 2844.31 Torr View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 34 p. 5441 - 5447
反应条件
in N,N-dimethyl-formamide
