(E)-4-十三碳烯-1-醇乙酸酯合成路线 （共 13 条）
反应条件
1: water; lithium chloride / dimethyl sulfoxide / 18 h / |Reflux
2: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / |Inert atmosphere
3: lithium aluminium tetrahydride / diethyl ether / 3 h / 20 °C / |Inert atmosphere
4: pyridine / diethyl ether / 1 h / 20 °C
View Scheme
参考文献
Shakhmaev; Sunagatullina; Zorin
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 5 p. 669 - 671
Zh. Org. Khim., 2013 , vol. 49, # 5 p. 687 - 689,3
反应条件
1: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / |Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 3 h / 20 °C / |Inert atmosphere
3: pyridine / diethyl ether / 1 h / 20 °C
View Scheme
参考文献
Shakhmaev; Sunagatullina; Zorin
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 5 p. 669 - 671
Zh. Org. Khim., 2013 , vol. 49, # 5 p. 687 - 689,3
反应条件
1: 1) Mg
2: 86 percent / pyridine
View Scheme
参考文献
Bikulova, L. M.; Verba, G. G.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1991 , vol. 27, # 3 p. 388
Khimiya Prirodnykh Soedinenii, 1990 , # 3 p. 444
