3,3-二甲基-1-苯基噻嗪合成路线 （共 30 条）
反应条件
sodium carbonate in water
T=5 - 10°C; 0.5 h;
参考文献
Ludwig, Miroslav; Valaskova, Pavla; Pytela, Oldrich
Collection of Czechoslovak Chemical Communications, 1994 , vol. 59, # 2 p. 401 - 411
反应条件
1: aniline With hydrogenchloride; sodium nitrite
T=0 - 10°C;
2: dimethyl amine With sodium carbonate in water
0.5 h; cooling;
参考文献
Manolov, Ilia; Machulla; Momekov
Pharmazie, 2006 , vol. 61, # 6 p. 511 - 516
反应条件
in dichloromethane
T=-30 - -20°C;
参考文献
Tyurin; Churakov; Ioffe; Strelenko; Tartakovsky
Russian Chemical Bulletin, 1997 , vol. 46, # 3 p. 592 - 594
反应条件
water
man reinigt durch Destillation in Vakuum;
参考文献
Baeyer; Jaeger
Chemische Berichte, 1875 , vol. 8, p. 151
反应条件
ethylmagnesium bromide
1.) THF, reflux, 10 min, 2.) THF, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Apasov, E. T.; Dzhetigenov, B. A.; Kalinin, A. V.; Tartakovskii, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 6.2 p. 1289 - 1291
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 6 p. 1450 - 1451
反应条件
T=90 - 100°C; Einleiten von HCl;
参考文献
Gen. Aniline and Film Corp.
Patent: US2280504 , 1939 ;
反应条件
buffer solution pH 1.2 in ethanol
T=37°C; μ=0.178; Rate constant;
参考文献
Nifontov, V. I.; Bel'skaya, N. P.; Chernov, V. A.; Ershova, Yu. A.; Validuda, G. I.; et al.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 9 p. 592 - 596
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 9 p. 1037 - 1041
参考文献
Gen. Aniline and Film Corp.
Patent: US2280504 , 1939 ;
参考文献
Gen. Aniline and Film Corp.
Patent: US2280504 , 1939 ;
反应条件
acetic acid; copper(l) chloride; sodium chloride; sulfur dioxide in water; acetone
T=10 - 15°C;
参考文献
Naidan; Smalius
Russian Journal of General Chemistry, 2004 , vol. 74, # 9 p. 1386 - 1388
