1-(4-硝基苯基)-3,3-二甲基三氮烯合成路线 (共 22 条)
反应条件
buffer solution pH 1.2 in ethanol T=37°C; μ=0.178; Rate constant;
参考文献
Nifontov, V. I.; Bel'skaya, N. P.; Chernov, V. A.; Ershova, Yu. A.; Validuda, G. I.; et al.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 9 p. 592 - 596
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 9 p. 1037 - 1041
反应条件
1: 4-nitro-aniline With hydrogenchloride; sodium nitrite
T=0 - 10°C;
2: dimethyl amine in water
cooling;
参考文献
Manolov, Ilia; Machulla; Momekov
Pharmazie, 2006 , vol. 61, # 6 p. 511 - 516
反应条件
sodium hydroxide
T=0 - 5°C; 0.5 h;
参考文献
Barbero; Degani; Diulgheroff; Dughera; Fochi
Synthesis, 2001 , # 14 p. 2180 - 2190
反应条件
1: 92 percent / NO2 / 6 h / 0 °C
2: 0 °C
View Scheme
参考文献
Kaupp, Gerd; Herrmann, Andreas
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 3 p. 256 - 260
参考文献
Kaupp, Gerd; Herrmann, Andreas
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 3 p. 256 - 260
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
water; sodium carbonate
参考文献
Elks; Hey
Journal of the Chemical Society, 1943 , p. 441,443
反应条件
Ambient temperature; Yield given;
参考文献
Kaupp, Gerd; Herrmann, Andreas
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 3 p. 256 - 260
参考文献
Hooper, Donald L.; Vaughan, Keith
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1161 - 1165
参考文献
Elks; Hey
Journal of the Chemical Society, 1943 , p. 441,443