1-(2-萘甲酰基 )乙醇合成路线 （共 127 条）
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; [(1,3-(2,6-iPr2C6H3)2-1,3-dihydroimidazol-2-ylidene)PdCl2]2 in 1,2-dichloro-ethane T=65°C; 20 h; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 5, # 1 p. 63 - 65
反应条件
α-naphthol; C136H102Fe2N4O6 in toluene T=50°C; 18 h; optical yield given as percent ee;
参考文献
Journal of the American Chemical Society, , vol. 133, # 33 p. 12937 - 12939
反应条件
lt;Mn3O(OAc)6(OAc)(HOAc)gt;*5H2O; lithium chloride in acetic acid 0.2 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 11 p. 3567 - 3571
反应条件
lt;Mn3O(OAc)6(OAc)(HOAc)gt;*5H2O; lithium chloride in acetic acid 0.2 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 11 p. 3567 - 3571
反应条件
HCOONa; [Cp*RhCl2]2; (1R,2R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine in water T=40°C; 4 h; Reactivity; Time; optical yield given as percent eeenantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 14, # 7 p. 2209 - 2222
反应条件
HCOONa; [Cp*RhCl2]2; (1R,2R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine in water T=40°C; 4 h; Reactivity; Time; optical yield given as percent eeenantioselective reaction;
参考文献
Wu, Xiaofeng; Li, Xiaohong; Zanotti-Gerosa, Antonio; Pettman, Allan; Liu, Jianke; Mills, Allan James; Xiao, Jianliang
Chemistry - A European Journal, 2008 , vol. 14, # 7 p. 2209 - 2222
反应条件
1: oxygen; (-)-sparteine; molecular sieves 3 Angstroem / [(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-yl)PdCl2]2 / 1,2-dichloro-ethane / 20 h / 65 °C 2: O2; (-)-sparteine / (Pd(IiPr)Cl2)2 / 1,2-dichloro-ethane / 20 h / 65 °C View Scheme
参考文献
Jensen, David R.; Sigman, Matthew S.
Organic Letters, 2003 , vol. 5, # 1 p. 63 - 65
反应条件
sulfuric acid in nitromethane
T=101°C; 0.0833333 h;
参考文献
Xia, Fei; Zhao, Zheng Le; Liu, Pei Nian
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2828 - 2832
反应条件
1: oxygen; (-)-sparteine; molecular sieves 3 Angstroem / [(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-yl)PdCl2]2 / 1,2-dichloro-ethane / 20 h / 65 °C
2: O2; (-)-sparteine / (Pd(IiPr)Cl2)2 / 1,2-dichloro-ethane / 20 h / 65 °C
View Scheme
参考文献
Jensen, David R.; Sigman, Matthew S.
Organic Letters, 2003 , vol. 5, # 1 p. 63 - 65
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; chlorobenzene; cesium fluoride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene
T=80°C; 1.5 h; Inert atmosphere;
参考文献
Berini, Christophe; Navarro, Oscar
Chemical Communications, 2012 , vol. 48, # 10 p. 1538 - 1540
