1-(2-萘甲酰基 )乙醇合成路线 (共 127 条)
反应条件
dichloro bis(acetonitrile) palladium(II); Ru2(CO)4(μ-H)(C4Ph4-COHOC-C4Ph4); water; p-benozquinone in methanol; isopropyl alcohol T=85°C; 36 h; Inert atmosphereGlovebox; regioselective reaction;
参考文献
Yang, Yongsheng; Guo, Jiayi; Ng, Huimin; Chen, Zhiyong; Teo, Peili
Chemical Communications, 2014 , vol. 50, # 20 p. 2608 - 2611
反应条件
in diethyl ether T=0 - 20°C; 2.5 h;
参考文献
Itoh, Toshiyuki; Matsushita, Yuichi; Abe, Yoshikazu; Han, Shi-Hui; Wada, Shohei; Hayase, Shuichi; Kawatsura, Motoi; Takai, Shigeomi; Morimoto, Minoru; Hirose, Yoshihiko
Chemistry - A European Journal, 2006 , vol. 12, # 36 p. 9228 - 9237
反应条件
in tetrahydrofuran T=-50°C; 4 h;
参考文献
Weidmann, Beat; Seebach, Dieter
Helvetica Chimica Acta, 1980 , vol. 63, # 8 p. 2451 - 2454
反应条件
sodium hydroxide in methanol; water T=20°C; 4 h;
参考文献
Letters in Organic Chemistry, , vol. 8, # 10 p. 690 - 695
反应条件
in diethyl ether T=20°C; 0.5 h;
参考文献
Krief, Alain; Clarembeau, M.; Barbeaux, Ph.
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 457 - 458
反应条件
in diethyl ether T=0°C; 2 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 5 p. 1250 - 1253
反应条件
in tetrahydrofuran T=-78°C; Grignard reaction; 5 h;
参考文献
Organic Letters, , vol. 7, # 4 p. 573 - 576
反应条件
1: methyl iodide With magnesium in diethyl ether Grignard reaction; 1 h; RefluxInert atmosphere; 2: β-naphthaldehyde in diethyl ether T=20 - 50°C; Grignard reaction; Ionic liquidInert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 5 p. 942 - 950
反应条件
water; sodium hydroxide in methanol; toluene T=50°C; 48 h;
参考文献
Organometallics, , vol. 30, # 17 p. 4720 - 4729
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 22, # 1 p. 93 - 98