1-(2-萘甲酰基 )乙醇合成路线 （共 127 条）
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 3.33333 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 46 p. 12780 - 12790
反应条件
4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; ammonium formate in methanol T=80°C; 4 h; chemoselective reaction;
参考文献
Chemistry - A European Journal, , vol. 20, # 1 p. 245 - 252
反应条件
4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline in ethyl acetate T=80°C; 4 h; chemoselective reaction;
参考文献
Chemistry - A European Journal, , vol. 20, # 1 p. 245 - 252
反应条件
1: diethylzinc With C56H43N2OP in toluene T=-35°C; 0.5 h; Inert atmosphere; 2: 2-acetonaphthalene in toluene T=-65°C; 96 h; Inert atmosphere;
参考文献
Dalton Transactions, , vol. 42, # 40 p. 14576 - 14582
反应条件
1: acetic acid / Heating 2: KOH / ethanol / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 22, # 1 p. 93 - 98
反应条件
in chloroform-d1 T=0 - 25°C; Product distribution / selectivity;
参考文献
US7741513 B2, ;
Page/Page column 15-16 ;
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 7 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
反应条件
1.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 7 h / 0 - 60 °C 2.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 2.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
反应条件
sodium hydroxide; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; dihydrogen peroxide; 1,4-di(diphenylphosphino)-butane; benzo[1,3,2]dioxaborole 1.) THF, 25 deg C, 16 h, 2.) THF, RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Asymmetry, , vol. 2, # 7 p. 601 - 612
反应条件
aluminium trichloride 1.) benzene, 30 deg C, 30 min, 2.) benzene, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthesis, , # 9 p. 1127 - 1130
