1-(2-萘甲酰基 )乙醇合成路线 （共 127 条）
反应条件
trimethyltelluronium iodide 1.) hexane, THF, -60 deg C, 10 min, 2.) -78 deg C -> RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2847 - 2848
反应条件
n-butyllithium 1.) hexane, THF, -60 deg C, 10 min, 2.) -78 deg C -> RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2847 - 2848
参考文献
Phytochemistry (Elsevier), , vol. 26, # 4 p. 1001 - 1004
反应条件
benzophenone in acetonitrile T=20°C; Inert atmosphereUV-irradiationPhotolysis; Quantum yield; Reagent/catalystConcentration;
参考文献
Heterocycles, , vol. 78, # 10 p. 2431 - 2437
反应条件
potassium tert-butylate; (CyRuCl2)2; (1R,2S)-1-amino-2,3-dihydro-1H-inden-2-ol in isopropyl alcohol; acetone T=25°C; 19 h; Title compound not separated from byproducts.;
参考文献
Faller; Lavoie, Adrien R.
Organic Letters, 2001 , vol. 3, # 23 p. 3703 - 3706
反应条件
C6mim(1+)Br(1-) T=140°C; 0.2 h; Microwave irradiationCombinatorial reaction / High throughput screening (HTS); chemoselective reaction;
参考文献
Kumar, Rakesh; Sharma, Abhishek; Sharma, Naina; Kumar, Vinod; Sinha, Arun K.
European Journal of Organic Chemistry, 2008 , # 33 p. 5577 - 5582
反应条件
graphene oxide in toluene T=65°C; 2 h; Sealed tubeInert atmosphere;
参考文献
RSC Advances, , vol. 3, # 44 p. 22130 - 22134
反应条件
1: SOCl2, Py / Heating 2: (i) NaOtBu, tBuOH, (ii) /BRN= 1935846/ 3: (i) KOH, H2O, (ii) (heating) 4: H3PO4, H2SO4 / acetic acid / 50 °C 5: (i) LiAlH4, Et2O, (ii) TsCl, Py, (iii) LiAlH4, Et2O 6: Pd-C / 330 - 340 °C View Scheme
参考文献
Regnault,A.; Canonne,P.
Tetrahedron, 1969 , vol. 25, p. 2349 - 2365
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; [(1,3-(2,6-iPr2C6H3)2-1,3-dihydroimidazol-2-ylidene)PdCl2]2 in 1,2-dichloro-ethane T=65°C; 20 h; Title compound not separated from byproducts.;
参考文献
Jensen, David R.; Sigman, Matthew S.
Organic Letters, 2003 , vol. 5, # 1 p. 63 - 65
反应条件
palladium dichloro (η-2,5-norbornadiene); oxygen; (-)-sparteine in toluene T=80°C; 112 h;
参考文献
Shiigi, Hirofumi; Mori, Hiroyuki; Tanaka, Tomoaki; Demizu, Yosuke; Onomura, Osamu
Tetrahedron Letters, 2008 , vol. 49, # 36 p. 5247 - 5251
