1-(2-萘甲酰基 )乙醇合成路线 （共 127 条）
反应条件
chiral 2-(3',5'-di-t-butylPh)-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 0.833333 h; Title compound not separated from byproducts;
参考文献
Crittall, Matthew R.; Rzepa, Henry S.; Carbery, David R.
Organic Letters, 2011 , vol. 13, # 5 p. 1250 - 1253
反应条件
Candida antarctica lipase (CAL) immobilized on BIO-M in di-isopropyl ether T=30°C; 0.5 h; Resolution of racemateMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Ema, Tadashi; Miyazaki, Yuki; Kozuki, Izumi; Sakai, Takashi; Hashimoto, Hideki; Takada, Jun
Green Chemistry, 2011 , vol. 13, # 11 p. 3187 - 3195
反应条件
potassium tert-butylate; (CyRuCl2)2; (1R,2S)-1-amino-2,3-dihydro-1H-inden-2-ol in isopropyl alcohol; acetone T=25°C; 19 h; Title compound not separated from byproducts.;
参考文献
Faller; Lavoie, Adrien R.
Organic Letters, 2001 , vol. 3, # 23 p. 3703 - 3706
反应条件
(1R,2R,4S,5S)-4,8,8-triMe-2-Ph-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
反应条件
chiral 2-(3',5'-di-t-butylPh)-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 0.366667 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
反应条件
(1R,2R,4S,5S)-4,8,8-triMe-2-Ph-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 0.916667 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
反应条件
chiral 2-(3',5'-di-t-butylPh)-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 75 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
反应条件
(1R,2R,4S,5S)-4,8,8-triMe-2-Ph-2-phosphabicyclo[3.3.0]octane in toluene T=20°C; 0.633333 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
参考文献
Collyer; Kenyon
Journal of the Chemical Society, 1940 , p. 676,678
反应条件
(S)-HBTM; N-ethyl-N,N-diisopropylamine in 1,1-dimethylpropan-1-ol; toluene T=-40°C; 5 h; optical yield given as percent ee;
参考文献
Belmessieri, Dorine; Joannesse, Caroline; Woods, Philip A.; MacGregor, Callum; Jones, Caroline; Campbell, Craig D.; Johnston, Craig P.; Duguet, Nicolas; Concellon, Carmen; Bragg, Ryan A.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 559 - 570
