1-甲氧基-9H-咔唑-3-甲醛合成路线 （共 24 条）
反应条件
1: caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl / toluene / 12 h / 96 °C
2: potassium carbonate; palladium diacetate; 2,2,2-trimethylacetic acid / 12 h / 115 °C
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参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH
Patent: US2012/202868 A1, 2012 ;
US 20120202868 A1
反应条件
manganese(IV) oxide
1) CH3CN, 46 h, RT, 2) toluene, RT 24 h and 2 d; Yield given. Multistep reaction;
参考文献
Knoelker, Hans-Joachim; Bauermeister, Michael
Tetrahedron, 1993 , vol. 49, # 48 p. 11221 - 11236
反应条件
manganese(IV) oxide; diisobutylaluminium hydride
Yield given. Multistep reaction;
参考文献
Knoelker, Hans-Joachim; Bauermeister, Michael
Tetrahedron, 1993 , vol. 49, # 48 p. 11221 - 11236
反应条件
Zn–Hg amalgam in ethanol
Heating;
参考文献
Benavides, Adriana; Peralta, Javier; Delgado, Francisco; Tamariz, Joaquin
Synthesis, 2004 , # 15 p. 2499 - 2504
