potassium carbonate in N,N-dimethyl-formamide
Alkylation; 72 h; Heating;
参考文献
Griffin, Jonathan L. W.; Coveney, Peter V.; Whiting, Andrew; Davey, Roger
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 10 p. 1973 - 1981
Vries, Erik F. J. de; Steenwinkel, Pablo; Brussee, Johannes; Kruse, Chris G.; Gen, Arne van der
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4315 - 4325
1: 75 percent / triethylamine / CH2Cl2 / 48 h / 5 °C
2: 1.) NaH / 1.) THF, mineral oil, reflux, 2 h, 2.) THF, reflux, 48 h
View Scheme
参考文献
Vries, Erik F. J. de; Steenwinkel, Pablo; Brussee, Johannes; Kruse, Chris G.; Gen, Arne van der
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4315 - 4325