1: 1,2-phenylenebis(methylphosphine) With potassium in ammonia
Metallation;
2: methyl iodide in tetrahydrofuran
Methylation; Title compound not separated from byproducts;
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
1.1: tetrahydrofuran
1.2: tetrahydrofuran / 96 h
View Scheme
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
1: 1,2-dichloro-benzene; (+/-)-(2-dimethylphosphinophenyl)methylphosphine in tetrahydrofuran
Alkylation;
2: 1,2-dichloro-benzene in tetrahydrofuran
Alkylation; 96 h; Further stages.;
参考文献
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
Chatterjee, Swarup; Doyle, Roy; Hockless, David C. R.; Salem, Geoffrey; Willis, Anthony C.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 12 p. 1829 - 1830
