(2-甲氧基苯基)-氧代乙腈合成路线 (共 10 条)
参考文献
Merck,E.
Patent: DE949521 , 1955 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=120°C; 12 h;
参考文献
Murahashi, Shun-Ichi; Naota, Takeshi; Nakajima, Nobuyuki
Journal of Organic Chemistry, 1986 , vol. 51, # 6 p. 898 - 901
反应条件
tert.-butylhydroperoxide; tris(triphenylphosphine)ruthenium(II) chloride in benzene
11 h; Ambient temperature;
参考文献
Murahashi; Naota
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 2 p. 203 - 213
反应条件
silver nitrate in acetonitrile
T=50°C; 5 h;
参考文献
Sueda, Takuya; Shoji, Masashi; Nishide, Kiyoharu
Tetrahedron Letters, 2008 , vol. 49, # 34 p. 5070 - 5072
反应条件
zinc(II) iodide
T=100°C; 2 h; Inert atmosphereNeat (no solvent)neat (no solvent);
参考文献
Zeng, Wei; Yang, Jingya; Meng, Bo; Zhang, Bo; Jiang, Mingzhe; Chen, Fu-Xue
Letters in Organic Chemistry, 2009 , vol. 6, # 8 p. 637 - 641
反应条件
1: 1.) NaHSO3
2: 82 percent / t-BuOOH / RuCl2(PPh3)3 / benzene / 11 h / Ambient temperature
View Scheme
参考文献
Murahashi, Shun-ichi; Naota, Takeshi; Nakajima, Nobuyuki
Tetrahedron Letters, 1985 , vol. 26, # 7 p. 925 - 928
反应条件
phosphorus pentoxide in xylene
Heating;
参考文献
Asinger,F. et al.
Justus Liebigs Annalen der Chemie, 1966 , vol. 691, p. 92 - 108
反应条件
1: thionyl chloride
2: pyridine
View Scheme
参考文献
Marsh; Stephen
Journal of the Chemical Society, 1925 , vol. 127, p. 1635
参考文献
Marsh; Stephen
Journal of the Chemical Society, 1925 , vol. 127, p. 1635
反应条件
water in acetonitrile
electrolysis at constant current 0.4 A in presence of Et4NOTs; in absence of H2O - 55percent;
参考文献
Okimoto, Mitsuhiro; Itoh, Toshiaki; Chiba, Toshiro
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4835 - 4837